Practical Isolation of the (1 R ,2 R )-Enantiomer from a Racemic cis/trans Mixture of 2-Methyl-1-cyclohexanamine

Posted by DaveB on octobre 17, 2017

Furegati, Nocito, Org. Process Res. Dev. 2017 [10.1021/acs.oprd.7b00263]

An Improved Synthesis of Amantadine Hydrochloride

Posted by DaveB on octobre 16, 2017

Vu, Nguyen, Le, Phan, Org. Process Res. Dev. 2017 [10.1021/acs.oprd.7b00242]

A Boron Protecting Group Strategy for 1,2-Azaborines

Posted by DaveB on octobre 11, 2017

Baggett, Liu, J. Am. Chem. Soc. 2017 [10.1021/jacs.7b09491]

Laser-Initiated Radical Trifluoromethylation of Peptides and Proteins: Application to Mass-Spectrometry-Based Protein Footprinting

Posted by DaveB on octobre 06, 2017

Cheng, Zhang, Cui, Gross, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201706697]

Esterification of Carboxylic Acids with Difluoromethyl Diazomethane and Interrupted Esterification with Trifluoromethyl Diazomethane: A Fluorine Effect

Posted by DaveB on octobre 05, 2017

Peng, Zhang, Zhang, Hu, Org. Lett. 2017 [10.1021/acs.orglett.7b02866]

1-Trifluoromethylisoquinolines from α-Benzylated Tosylmethyl Isocyanide Derivatives in a Modular Approach

Posted by DaveB on octobre 04, 2017

Wang, Studer, Org. Lett. 2017 [10.1021/acs.orglett.7b02882]

Remote, Late-Stage Oxidation of Aliphatic C–H Bonds in Amide-Containing Molecules

Posted by DaveB on octobre 04, 2017

Nanjo, De Lucca, White, J. Am. Chem. Soc. 2017 [10.1021/jacs.7b07665]

Ligand-Promoted Palladium-Catalyzed Aerobic Oxidation Reactions

Posted by DaveB on octobre 04, 2017

Wang, Weinstein, White, Stahl, Chem. Rev. 2017 [10.1021/acs.chemrev.7b00334]

Nickel(II)-Catalyzed Site-Selective C–H Bond Trifluoromethylation of Arylamine in Water through a Coordinating Activation Strategy

Posted by DaveB on octobre 02, 2017

Xu, Qiao, Shen, Chai, Shen, Zhang, Org. Lett. 2017 [10.1021/acs.orglett.7b02823]

Oxidative Synthesis of Benzimidazoles, Quinoxalines, and Benzoxazoles from Primary Amines by ortho -Quinone Catalysis

Posted by DaveB on octobre 02, 2017

Zhang, Qin, Zhang, Luo, Org. Lett. 2017 [10.1021/acs.orglett.7b02786]

Metal- and Solvent-Free Approach to Diversely Substituted Picolinates via Domino Reaction of Cyclic Sulfamidate Imines with β,γ-Unsaturated α-Ketocarbonyls

Posted by DaveB on octobre 02, 2017

Biswas, Majee, Guin, Samanta, J. Org. Chem. 2017 [10.1021/acs.joc.7b01792]

A practical and scalable system for heteroaryl amino acid synthesis

Posted by DaveB on octobre 02, 2017

Aycock, Vogt, Jui, Chem. Sci. 2017 [10.1039/C7SC03612D]

Design, Synthesis, and Application of Polymer-Supported Silicon-Transfer Agents for Cross-Coupling Reactions with Organolithium Reagents

Posted by DaveB on octobre 02, 2017

Nguyen, O’brien, Smith, J. Org. Chem. 2017 [10.1021/acs.joc.7b02004]

Difluorocarbene for Dehydroxytrifluoromethylthiolation of Alcohols

Posted by DaveB on septembre 29, 2017

Luo, Zhang, Lin, Xiao, J. Org. Chem. 2017 [10.1021/acs.joc.7b01701]

Learning Medicinal Chemistry Absorption, Distribution, Metabolism, Excretion, and Toxicity (ADMET) Rules from Cross-Company Matched Molecular Pairs Analysis (MMPA)

Posted by DaveB on septembre 28, 2017

Kramer, Ting, Zheng, Hert, Schindler, Stahl, Robb, Crawford, Blaney, Montague, Leach, Dossetter, Griffen, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00935]

Manganese-Based Photoredox Catalysis for C-H Alkylation of Heteroarenes: Applications and Mechanistic Studies

Posted by DaveB on septembre 28, 2017

Oderinde, Nuhant, Genovino, Juneau, Gagné, Allais, Chinigo, Choi, Sach, Bernier, Bundesmann, Khunte, Frenette, Fadeyi, Fobian, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201707958]

Photoredox Enables the Construction of 1,1-Difluoroalkene Carbonyl Mimics

Posted by DaveB on septembre 28, 2017

Molander, Lang, Wiles, Kelly, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201709487]

Beyond the Rule of 5: Lessons Learned from AbbVie’s Drugs and Compound Collection

Posted by DaveB on septembre 27, 2017

Degoey, Chen, Cox, Wendt, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00717]

Discovery of a Potent and Specific M. tuberculosis Leucyl-tRNA Synthetase Inhibitor: ( S )-3-(Aminomethyl)-4-chloro-7-(2-hydroxyethoxy)benzo[ c ][1,2]oxaborol-1(3 H )-ol (GSK656)

Posted by DaveB on septembre 27, 2017

Li, Hernandez, Rock, Choi, Mak, Mohan, Mao, Zhou, Easom, Plattner, Zou, Pérez-herrán, Giordano, Mendoza-losana, Alemparte, Rullas, Angulo-barturen, Crouch, Ortega, Barros, Alley, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00631]

Synthesis of Bicyclic Isothiazoles through an Intramolecular Rhodium-Catalyzed Transannulation of Cyanothiadiazoles

Posted by DaveB on septembre 25, 2017

Seo, Kim, Kim, Baek, Um, Lee, J. Org. Chem. 2017, 82(19), 10574-10582 [10.1021/acs.joc.7b02077]

Synthetic nat- or ent-steroids in as few as five chemical steps from epichlorohydrin

Posted by DaveB on septembre 25, 2017

Kim, Du, Eastman, Hughes, Micalizio, Nat. Chem. 2017 [10.1038/nchem.2865]

An Aminocatalyzed Michael Addition/Iron-Mediated Decarboxylative Cyclization Sequence for the Preparation of 2,3,4,6-Tetrasubstituted Pyridines: Scope and Mechanistic Insights

Posted by DaveB on septembre 22, 2017

Stivanin, Duarte, Sartori, Capreti, Angolini, Jurberg, J. Org. Chem. 2017, 82(19), 10319-10330 [10.1021/acs.joc.7b01789]

Reaction dynamics: The view from a transition state

Posted by DaveB on septembre 22, 2017

Continetti, Nat. Chem. 2017, 9(10), 931-932 [10.1038/nchem.2868]

Modular Access to Triarylethylene Units from Arylvinyl MIDA Boronates Using a Regioselective Heck Coupling

Posted by DaveB on septembre 22, 2017

Khanizeman, Barde, Bates, Guérinot, Cossy, Org. Lett. 2017, 19(19), 5046-5049 [10.1021/acs.orglett.7b02218]

Joining Forces: The Chemical Biology–Medicinal Chemistry Continuum

Posted by DaveB on septembre 21, 2017

Plowright, Ottmann, Arkin, Auberson, Timmerman, Waldmann, Cell Chemical Biology 2017, 24(9), 1058-1065 [10.1016/j.chembiol.2017.05.019]

Intermolecular Radical Addition to Carbonyls Enabled by Visible Light Photoredox Initiated Hole Catalysis

Posted by DaveB on septembre 21, 2017

Pitzer, Sandfort, Strieth-kalthoff, Glorius, J. Am. Chem. Soc. 2017, 139(39), 13652-13655 [10.1021/jacs.7b08086]

Radical heterocyclization and heterocyclization cascades triggered by electron transfer to amide-type carbonyls

Posted by DaveB on septembre 20, 2017

Huang, Procter, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201708354]

One-pot, Three-Component Sulfonimidamide Synthesis exploiting the Sulfinylamine Reagent N-Sulfinyltritylamine, TrNSO

Posted by DaveB on septembre 20, 2017

Davies, Hall, Willis, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201708590]

Visible-Light-Promoted C–S Cross-Coupling via Intermolecular Charge Transfer

Posted by DaveB on septembre 19, 2017

Liu, Lim, Miyake, J. Am. Chem. Soc. 2017, 139(39), 13616-13619 [10.1021/jacs.7b07390]

Pyruvate Enolate Arylation and Alkylation: OBO Ester Protected Pyruvates as Useful Reagents in Organic Synthesis

Posted by DaveB on septembre 18, 2017

Alves Esteves, Hall, Smith, Donohoe, Org. Lett. 2017, 19(19), 5248-5251 [10.1021/acs.orglett.7b02524]

Ketones as directing groups in photocatalytic sp 3 C–H fluorination

Posted by DaveB on septembre 17, 2017

Bume, Pitts, Ghorbani, Harry, Capilato, Siegler, Lectka, Chem. Sci. 2017 [10.1039/C7SC02703F]

Difluoromethylation of Carboxylic Acids via the Addition of Difluorinated Phosphorus Ylide to Acyl Chlorides

Posted by DaveB on septembre 15, 2017

Trifonov, Levin, Struchkova, Dilman, Org. Lett. 2017 [10.1021/acs.orglett.7b02601]

Exploiting a “Beast” in Carbenoid Chemistry: Development of a Straightforward Direct Nucleophilic Fluoromethylation Strategy

Posted by DaveB on septembre 15, 2017

Parisi, Colella, Monticelli, Romanazzi, Holzer, Langer, Degennaro, Pace, Luisi, J. Am. Chem. Soc. 2017 [10.1021/jacs.7b07891]

The photochemical alkylation and reduction of heteroarenes

Posted by DaveB on septembre 15, 2017

Mccallum, Pitre, Morin, Scaiano, Barriault, Chem. Sci. 2017 [10.1039/C7SC03768F]

The Application of a Continuous Grignard Reaction in the Preparation of Fluconazole

Posted by DaveB on septembre 15, 2017

Gupton, Korwar, Amir, Tosso, Kong, Fadnis, Desai, Ahmad, Telang, Roper, Eur. J. Org. Chem. 2017 [10.1002/ejoc.201701002]

Recent Advances in the Chemical Synthesis of C -Glycosides

Posted by DaveB on septembre 15, 2017

Yang, Yu, Chem. Rev. 2017 [10.1021/acs.chemrev.7b00234]

Stereoselective Synthesis of Nitrogen-Containing Compounds from Enamines

Posted by DaveB on septembre 15, 2017

Sugiura, Kashiwagi, Ito, Kotani, Nakajima, J. Org. Chem. 2017 [10.1021/acs.joc.7b01923]

Lab-scale production of anhydrous diazomethane using membrane separation technology

Posted by DaveB on septembre 14, 2017

Dallinger, Kappe, Nature Protocols 2017, 12(10), 2138-2147 [10.1038/nprot.2017.046]

Electrochemically Enabled, Nickel-Catalyzed Amination

Posted by DaveB on septembre 14, 2017

Li, Kawamata, Nakamura, Vantourout, Liu, Hou, Bao, Starr, Chen, Yan, Baran, Angew. Chem. Int. Ed. 2017, 56(42), 13088-13093 [10.1002/anie.201707906]

Ex Situ Generation of Sulfuryl Fluoride for the Synthesis of Aryl Fluorosulfates

Posted by DaveB on septembre 13, 2017

Veryser, Demaerel, Bieliunas, Gilles, De Borggraeve, Org. Lett. 2017 [10.1021/acs.orglett.7b02522]

Visible-Light-Enabled Decarboxylative Mono- and Difluoromethylation of Cinnamic Acids under Metal-Free Conditions

Posted by DaveB on septembre 13, 2017

Tang, Feng, Xu, Cheng, Xu, Dai, Xu, Org. Lett. 2017 [10.1021/acs.orglett.7b02129]

The Direct C–H Difluoromethylation of Heteroarenes Based on the Photolysis of Hypervalent Iodine(III) Reagents That Contain Difluoroacetoxy Ligands

Posted by DaveB on septembre 12, 2017

Sakamoto, Kashiwagi, Maruoka, Org. Lett. 2017 [10.1021/acs.orglett.7b02416]

Natural-Products-Inspired Use of the gem -Dimethyl Group in Medicinal Chemistry

Posted by DaveB on septembre 12, 2017

Talele, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00315]

Pd-PEPPSI-IPent-SiO2, a Supported Catalyst for Challenging Negishi Coupling Reactions in Flow

Posted by DaveB on septembre 12, 2017

Organ, Price, Hassan, Bogdan, Djuric, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201708598]

Tertiary Amine Synthesis via Reductive Coupling of Amides with Grignard Reagents

Posted by DaveB on septembre 11, 2017

Dixon, Xie, Chem. Sci. 2017 [10.1039/C7SC03613B]

Fluoroalkyl Amino Reagents for the Introduction of the Fluoro(trifluoromethoxy)methyl Group onto Arenes and Heterocycles

Posted by DaveB on septembre 04, 2017

Schmitt, Bouvet, Pégot, Panossian, Vors, Pazenok, Magnier, Leroux, Org. Lett. 2017, 19(18), 4960-4963 [10.1021/acs.orglett.7b02444]

Catalytic Enantioselective Synthesis of Highly Functionalized Difluoromethylated Cyclopropanes

Posted by DaveB on septembre 01, 2017

Bos, Huang, Poisson, Pannecoucke, Charette, Jubault, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201707375]

Silver-Catalyzed Decarboxylative Trifluoromethylation of Aliphatic Carboxylic Acids

Posted by DaveB on août 30, 2017

Tan, Liu, Shen, Zhang, Zhang, Li, J. Am. Chem. Soc. 2017, 139(36), 12430-12433 [10.1021/jacs.7b07944]

The Synthesis of Trifluoromethyl-sulfonimidamides from Sulfinamides

Posted by DaveB on août 30, 2017

Richards-taylor, Martínez-lamenca, Leenaerts, Trabanco, Oehlrich, J. Org. Chem. 2017, 82(18), 9898-9904 [10.1021/acs.joc.7b01628]

Nickel-Catalyzed Defluorinative Reductive Cross-Coupling of gem -Difluoroalkenes with Unactivated Secondary and Tertiary Alkyl Halides

Posted by DaveB on août 29, 2017

Lu, Wang, Zhang, Pi, Wang, Gong, Xiao, Fu, J. Am. Chem. Soc. 2017, 139(36), 12632-12637 [10.1021/jacs.7b06469]

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