Direct Difluoromethylenation of Carbonyl Compounds Using TMSCF3: The Right Conditions

Posted by DaveB on août 26, 2016

Prakash, Krishnamoorthy, Kothandaraman, Saldana, Eur. J. Org. Chem. 2016, online publication [10.1002/ejoc.201601038]

Role of LiCl in Generating Soluble Organozinc Reagents

Posted by DaveB on août 25, 2016

Feng, Cunningham, Easter, Blum, J. Am. Chem. Soc. 2016, online publication [10.1021/jacs.6b08465]

Rapid Synthesis of Aryl Fluorides in Continuous Flow through the Balz-Schiemann Reaction

Posted by DaveB on août 25, 2016

Park, Senter, Buchwald, Angew. Chem. Int. Ed. 2016, online publication [10.1002/anie.201606601]

Bis(difluoromethyl)trimethylsilicate Anion: A Key Intermediate in Nucleophilic Difluoromethylation of Enolizable Ketones with Me3SiCF2H

Posted by DaveB on août 24, 2016

Chen, Ni, Zhao, Cai, Li, Xiao, Hu, Angew. Chem. Int. Ed. 2016, online publication [10.1002/anie.201605280]

Complementary Methods for the Introduction of the ( E )-3-(Pentafluorosulfanyl)allyl Chain unto O-, N-, S-, and C-Based Nucleophiles

Posted by DaveB on août 23, 2016

Desroches, Forcellini, Paquin, Eur. J. Org. Chem. 2016, online publication [10.1002/ejoc.201600684]

Synthesis and Applications of Fluorocyclopropanes

Posted by DaveB on août 16, 2016

Pons, Poisson, Pannecoucke, Charette, Jubault, Synthesis 2016, online publication [10.1055/s-0035-1560557]

A Homogeneous Method for the Conveniently Scalable Palladium- and Nickel-Catalyzed Cyanation of Aryl Halides

Posted by DaveB on août 01, 2016

Burg, Egger, Deutsch, Guimond, Organic Process Research & Development 2016, 20(8), 1540-1545 [10.1021/acs.oprd.6b00229]

Fluorodecarboxylation for the Synthesis of Trifluoromethyl Aryl Ethers

Posted by DaveB on juillet 07, 2016

Zhang, Brusoe, Mascitti, Hesp, Blakemore, Kohrt, Hartwig, Angew. Chem. Int. Ed. 2016, 55(33), 9758-9762 [10.1002/anie.201604793]

Catalytic, asymmetric difluorination of alkenes to generate difluoromethylated stereocenters

Posted by DaveB on juillet 01, 2016

Banik, Medley, Jacobsen, Science 2016, 353(6294), 51-54 [10.1126/science.aaf8078]

Unexpected Reactivity of Trifluoromethyl Diazomethane (CF 3 CHN 2 ): Electrophilicity of the Terminal N-Atom

Posted by DaveB on juin 28, 2016

Arkhipov, Arkhipov, Cossy, Kovtunenko, Mykhailiuk, Org. Lett. 2016, 18(14), 3406-3409 [10.1021/acs.orglett.6b01565]

Abstract Image

Direct Access to α,α-Difluoroacylated Arenes by Palladium-Catalyzed Carbonylation of (Hetero)Aryl Boronic Acid Derivatives

Posted by DaveB on juin 27, 2016

Andersen, Frederiksen, Domino, Skrydstrup, Angew. Chem. Int. Ed. 2016, 55(35), 10396-10400 [10.1002/anie.201604152]

Siladifluoromethylation and Difluoromethylation onto C(sp 3 ), C(sp 2 ), and C(sp) Centers Using Ruppert–Prakash Reagent and Fluoroform

Posted by DaveB on juin 24, 2016

Aikawa, Maruyama, Nitta, Hashimoto, Mikami, Org. Lett. 2016, 18(14), 3354-3357 [10.1021/acs.orglett.6b01476]

Abstract Image

Nucleophilic Difluoromethylation Using (Bromodifluoromethyl)trimethylsilane

Posted by DaveB on juin 23, 2016

Trifonov, Zemtsov, Levin, Struchkova, Dilman, Org. Lett. 2016, 18(14), 3458-3461 [10.1021/acs.orglett.6b01641]

Abstract Image

Regioselective 2,2,2-Trifluoroethylation of Imidazopyridines by Visible Light Photoredox Catalysis

Posted by DaveB on juin 22, 2016

Zhu, Han, Fu, Wang, Ji, Hao, Song, Xu, J. Org. Chem. 2016, 81(16), 7282-7287 [10.1021/acs.joc.6b00950]

Abstract Image

Single C−F Bond Cleavage of Trifluoromethylarenes with an ortho -Silyl Group

Posted by DaveB on juin 17, 2016

Yoshida, Shimomori, Kim, Hosoya, Angew. Chem. Int. Ed. 2016, 55(35), 10406-10409 [10.1002/anie.201604776]

Yoshida, Shimomori, Kim, Hosoya, Angew. Chem. Int. Ed. 2016, 55(35), 10406-10409 [10.1002/anie.201604776]

http://onlinelibrary.wiley.com/store/10.1002/anie.201604776/asset/image_m/anie201604776-toc-0001-m.png?v=1&s=4d99b9244f7194e85b315f7676b28fcec03e5b27

Palladium Catalysis Enables Benzylation of α,α-Difluoroketone Enolates

Posted by DaveB on juin 17, 2016

Yang, Hunt, Sharifi, Altman, Angew. Chem. Int. Ed. 2016, 55(31), 9080-9083 [10.1002/anie.201604149]

Direct Difluoromethylation of Alcohols with an Electrophilic Difluoromethylated Sulfonium Ylide

Posted by DaveB on juin 17, 2016

Zhu, Liu, Shen, Angew. Chem. Int. Ed. 2016, 55(31), 9050-9054 [10.1002/anie.201603166]

Site-Selective Tertiary Alkyl-Fluorine Bond Formation from α-Bromoamides Using a Copper/CsF Catalyst System

Posted by DaveB on juin 10, 2016

Nishikata, Ishida, Fujimoto, Angew. Chem. Int. Ed. 2016, 55(34), 10008-10012 [10.1002/anie.201603426]

Preparative Scale Demonstration and Mechanistic Investigation of a Visible Light-Mediated Radical Smiles Rearrangement

Posted by DaveB on juin 01, 2016

Douglas, Sevrin, Cole, Stephenson, Organic Process Research & Development 2016, 20(7), 1148-1155 [10.1021/acs.oprd.6b00126]

Abstract Image

Trifluoromethylation of Arylsilanes with [(phen)CuCF3]

Posted by DaveB on mai 23, 2016

Morstein, Hou, Cheng, Hartwig, Angew. Chem. Int. Ed. 2016, 55(28), 8054-8057 [10.1002/anie.201601163]


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