Development of (Trifluoromethyl)zinc Reagent as Trifluoromethyl Anion and Difluorocarbene Sources

Posted by DaveB on octobre 02, 2015

Aikawa, Toya, Nakamura, Mikami, Org. Lett. 2015, ASAP [10.1021/acs.orglett.5b02439]

ol-2015-024399_0010[1]

In-Depth Assessment of the Palladium-Catalyzed Fluorination of Five-Membered Heteroaryl Bromides

Posted by DaveB on octobre 02, 2015

Milner, Yang, Buchwald, Organometallics 2015, ASAP [10.1021/acs.organomet.5b00631]

organomet5b00631-1

organomet5b00631-2.gif

A Fluorinated Ligand Enables Room Temperature and Regioselective Pd-Catalyzed Fluorination of Aryl Triflates and Bromides

Posted by DaveB on octobre 02, 2015

Sather, Lee, De La Rosa, Yang, Müller, Buchwald, J. Am. Chem. Soc. 2015, ASAP [10.1021/jacs.5b09308]

jacs5b09308-1

jacs5b09308-2

In Situ Generated Fluorinated Iminium Salts for Difluoromethylation and Difluoroacetylation

Posted by DaveB on septembre 05, 2015

Schmitt, Rugeri, Panossian, Vors, Pazenok, Leroux, Org. Lett. 2015, 17(18), 4510-4513 [10.1021/acs.orglett.5b02184]

ol-2015-021847_0012[1]

Synthesis of 1,4,2-Oxathiazoles via Oxidative Cyclization of Thiohydroximic Acids

Posted by DaveB on septembre 02, 2015

Lemercier, Pierce, Org. Lett. 2015, 17(18), 4542-4545 [10.1021/acs.orglett.5b02256]

ol-2015-02256s_0007[1]

Hydrodecarboxylation of Carboxylic and Malonic Acid Derivatives via Organic Photoredox Catalysis: Substrate Scope and Mechanistic Insight

Posted by DaveB on août 28, 2015

Griffin, Zeller, Nicewicz, J. Am. Chem. Soc. 2015, 137(35), 11340-11348 [10.1021/jacs.5b07770]

ja-2015-07770j_0017[1]

Transition-Metal-Free Cross-Coupling of Aryl and N-Heteroaryl Cyanides with Benzylic Zinc Reagents

Posted by DaveB on août 27, 2015

Quinio, Roman, León, William, Karaghiosoff, Knochel, Org. Lett. 2015, 17(17), 4396-4399 [10.1021/acs.orglett.5b02380]

ol-2015-023802_0008[1]

Nucleophilic Iododifluoromethylation of Aldehydes Using Bromine/Iodine Exchange

Posted by DaveB on août 24, 2015

Levin, Smirnov, Struchkova, Dilman, J. Org. Chem. 2015, 80(18), 9349-9353 [10.1021/acs.joc.5b01590]

jo-2015-01590y_0008[1]

Stereospecific Coupling of Boronic Esters with N-Heteroaromatic Compounds

Posted by DaveB on août 22, 2015

Llaveria, Leonori, Aggarwal, J. Am. Chem. Soc. 2015, 137(34), 10958-10961 [10.1021/jacs.5b07842]

ja-2015-07842q_0007[1]

General Ambient Temperature Benzylic Metalations Using Mixed-Metal Li/K-TMP Amide

Posted by DaveB on août 21, 2015

Manvar, Fleming, O’shea, J. Org. Chem. 2015, 80(17), 8727-8738 [10.1021/acs.joc.5b01540]

jo-2015-015406_0012[1]

Unexpected Mild Protection of Alcohols as 2-O-THF and 2-O-THP Ethers Catalysed by Cp2TiCl Reveal an Intriguing Role of the Solvent in the Single-Electron Transfer Reaction

Posted by DaveB on août 20, 2015

Durán-peña, Botubol-ares, Hanson, Hernández-galán, Collado, European Journal of Organic Chemistry 2015, 2015(28), 6333-6340 [10.1002/ejoc.201500869]

ejoc201500869

Direct Transformation of Esters into Arenes with 1,5-Bifunctional Organomagnesium Reagents

Posted by DaveB on août 20, 2015

Link, Fischer, Sparr, Angew. Chem. Int. Ed. 2015, 54(41), 12163-12166 [10.1002/anie.201505414]

acie201505414

Access to Highly Substituted 7-Azaindoles from 2-Fluoropyridines via 7-Azaindoline Intermediates

Posted by DaveB on août 20, 2015

Nuhant, Allais, Chen, Coe, Dermenci, Fadeyi, Flick, Mousseau, Org. Lett. 2015, 17(17), 4292-4295 [10.1021/acs.orglett.5b02098]

ol-2015-02098g_0011[2]

Kinetic Profiling of Catalytic Organic Reactions as a Mechanistic Tool

Posted by DaveB on août 18, 2015

Blackmond, J. Am. Chem. Soc. 2015, 137(34), 10852-10866 [10.1021/jacs.5b05841]

ja-2015-05841m_0029[1]

N-Difluoromethylthiophthalimide: A Shelf-Stable, Electrophilic Reagent for Difluoromethylthiolation

Posted by DaveB on août 18, 2015

Zhu, Gu, Lu, Shen, J. Am. Chem. Soc. 2015, , 150818092125007 [10.1021/jacs.5b03170]

ja-2015-03170r_0007[1]

Copper-Catalyzed Synthesis of Trifluoroethylarenes from Benzylic Bromodifluoroacetates

Posted by DaveB on août 11, 2015

Ambler, Zhu, Altman, J. Org. Chem. 2015, 80(16), 8449-8457 [10.1021/acs.joc.5b01343]

jo-2015-013434_0009[1]

Synthesis of Vinyl Chlorides via Triphosgene–Pyridine Activation of Ketones

Posted by DaveB on août 06, 2015

Saputra, Ngo, Kartika, J. Org. Chem. 2015, 80(17), 8815-8820 [10.1021/acs.joc.5b01137]

jo-2015-01137c_0007[2]

Photoredox Cross-Coupling: Ir/Ni Dual Catalysis for the Synthesis of Benzylic Ethers

Posted by DaveB on juin 16, 2015

Karakaya, Primer, Molander, Org. Lett. 2015, 17(13), 3294-3297 [10.1021/acs.orglett.5b01463]

ol-2015-014632_0005[3]

Selective Monoarylation of Primary Amines Using the Pd-PEPPSI-IPent Cl Precatalyst

Posted by DaveB on juin 10, 2015

Sharif, Rucker, Chandrasoma, Mitchell, Rodriguez, Froese, Organ, Angew. Chem. Int. Ed. 2015, 54(33), 9507-9511 [10.1002/anie.201502822]

acie201502822

2-Naphthylmethoxymethyl as a Mildly Introducible and Oxidatively Removable Benzyloxymethyl-Type Protecting Group

Posted by DaveB on juin 03, 2015

Sato, Oishi, Torikai, Org. Lett. 2015, 17(12), 3110-3113 [10.1021/acs.orglett.5b01408]

ol-2015-01408q_0007[1]


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