Ketones as directing groups in photocatalytic sp 3 C–H fluorination

Posted by DaveB on septembre 17, 2017

Bume, Pitts, Ghorbani, Harry, Capilato, Siegler, Lectka, Chem. Sci. 2017 [10.1039/C7SC02703F]

Difluoromethylation of Carboxylic Acids via the Addition of Difluorinated Phosphorus Ylide to Acyl Chlorides

Posted by DaveB on septembre 15, 2017

Trifonov, Levin, Struchkova, Dilman, Org. Lett. 2017 [10.1021/acs.orglett.7b02601]

Exploiting a “Beast” in Carbenoid Chemistry: Development of a Straightforward Direct Nucleophilic Fluoromethylation Strategy

Posted by DaveB on septembre 15, 2017

Parisi, Colella, Monticelli, Romanazzi, Holzer, Langer, Degennaro, Pace, Luisi, J. Am. Chem. Soc. 2017 [10.1021/jacs.7b07891]

The photochemical alkylation and reduction of heteroarenes

Posted by DaveB on septembre 15, 2017

Mccallum, Pitre, Morin, Scaiano, Barriault, Chem. Sci. 2017 [10.1039/C7SC03768F]

The Application of a Continuous Grignard Reaction in the Preparation of Fluconazole

Posted by DaveB on septembre 15, 2017

Gupton, Korwar, Amir, Tosso, Kong, Fadnis, Desai, Ahmad, Telang, Roper, Eur. J. Org. Chem. 2017 [10.1002/ejoc.201701002]

Recent Advances in the Chemical Synthesis of C -Glycosides

Posted by DaveB on septembre 15, 2017

Yang, Yu, Chem. Rev. 2017 [10.1021/acs.chemrev.7b00234]

Ex Situ Generation of Sulfuryl Fluoride for the Synthesis of Aryl Fluorosulfates

Posted by DaveB on septembre 13, 2017

Veryser, Demaerel, Bieliunas, Gilles, De Borggraeve, Org. Lett. 2017 [10.1021/acs.orglett.7b02522]

Visible-Light-Enabled Decarboxylative Mono- and Difluoromethylation of Cinnamic Acids under Metal-Free Conditions

Posted by DaveB on septembre 13, 2017

Tang, Feng, Xu, Cheng, Xu, Dai, Xu, Org. Lett. 2017 [10.1021/acs.orglett.7b02129]

The Direct C–H Difluoromethylation of Heteroarenes Based on the Photolysis of Hypervalent Iodine(III) Reagents That Contain Difluoroacetoxy Ligands

Posted by DaveB on septembre 12, 2017

Sakamoto, Kashiwagi, Maruoka, Org. Lett. 2017 [10.1021/acs.orglett.7b02416]

Laboratory-scale photoredox catalysis using hydrated electrons sustainably generated with a single green laser

Posted by DaveB on septembre 12, 2017

Naumann, Kerzig, Goez, Chem. Sci. 2017 [10.1039/C7SC03514D]

Natural-Products-Inspired Use of the gem -Dimethyl Group in Medicinal Chemistry

Posted by DaveB on septembre 12, 2017

Talele, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00315]

Pd-PEPPSI-IPent-SiO2, a Supported Catalyst for Challenging Negishi Coupling Reactions in Flow

Posted by DaveB on septembre 12, 2017

Organ, Price, Hassan, Bogdan, Djuric, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201708598]

Tertiary Amine Synthesis via Reductive Coupling of Amides with Grignard Reagents

Posted by DaveB on septembre 11, 2017

Dixon, Xie, Chem. Sci. 2017 [10.1039/C7SC03613B]

Chlorodifluoromethane-triggered formation of difluoromethylated arenes catalysed by palladium

Posted by DaveB on septembre 08, 2017

Feng, Min, Fu, An, Zhang, Nat. Chem. 2017, 9(9), 918-923 [10.1038/NCHEM.2746]

Catalytic Enantioselective Synthesis of Highly Functionalized Difluoromethylated Cyclopropanes

Posted by DaveB on septembre 01, 2017

Bos, Huang, Poisson, Pannecoucke, Charette, Jubault, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201707375]

Silver-Catalyzed Decarboxylative Trifluoromethylation of Aliphatic Carboxylic Acids

Posted by DaveB on août 30, 2017

Tan, Liu, Shen, Zhang, Zhang, Li, J. Am. Chem. Soc. 2017, 139(36), 12430-12433 [10.1021/jacs.7b07944]

The Synthesis of Trifluoromethyl-sulfonimidamides from Sulfinamides

Posted by DaveB on août 30, 2017

Richards-taylor, Martínez-lamenca, Leenaerts, Trabanco, Oehlrich, J. Org. Chem. 2017, 82(18), 9898-9904 [10.1021/acs.joc.7b01628]

Nickel-Catalyzed Defluorinative Reductive Cross-Coupling of gem -Difluoroalkenes with Unactivated Secondary and Tertiary Alkyl Halides

Posted by DaveB on août 29, 2017

Lu, Wang, Zhang, Pi, Wang, Gong, Xiao, Fu, J. Am. Chem. Soc. 2017, 139(36), 12632-12637 [10.1021/jacs.7b06469]

Synthetic Organic Electrochemistry: Calling All Engineers

Posted by DaveB on août 29, 2017

Recently noted this interesting call advocating for more efforts in democratizing electrochemistry…

Yan, Kawamata, Baran, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201707584]

But this seems to be superseeded now, since the announcement of this device, developed by IKA in a collaboration with the Baran group:

Future will tell us if this solves the main hurdles to the development of robust methodologies in this field…

Recent Developments in the Deoxyfluorination of Alcohols and Phenols: New Reagents, Mechanistic Insights, and Applications

Posted by DaveB on août 28, 2017

Hu, Hu, Hunter, Synthesis 2017 [10.1055/s-0036-1590881]

Copper-Catalyzed C–N Bond Exchange of N-Heterocyclic Substituents around Pyridine and Pyrimidine Cores

Posted by DaveB on août 28, 2017

Tao, Ji, Shi, Liu, Xu, Dai, Synthesis 2017 [10.1055/s-0036-1590893]

Sequential O-Arylation/Lanthanide(III)-Catalyzed [3,3]-Sigmatropic Rearrangement of Bromo-Substituted Allylic Alcohols

Posted by DaveB on août 25, 2017

Ramadhar, Kawakami, Batey, Synlett 2017 [10.1055/s-0036-1590890]

Photochemical Synthesis of 3-Azabicyclo[3.2.0]heptanes: Advanced Building Blocks for Drug Discovery

Posted by DaveB on août 25, 2017

Denisenko, Druzhenko, Skalenko, Samoilenko, Grygorenko, Zozulya, Mykhailiuk, J. Org. Chem. 2017, 82(18), 9627-9636 [10.1021/acs.joc.7b01678]

An Update on Direct C–H Bond Functionalization of Nitrogen-Containing Fused Heterocycles

Posted by DaveB on août 25, 2017

Aziz, Piguel, Synthesis 2017 [10.1055/s-0036-1590859]

4-Ethoxy-1,1,1-trifluoro-3-buten-2-one (ETFBO), a Versatile Precursor for Trifluoromethyl-Substituted Heteroarenes – a Short Synthesis of Celebrex® (Celecoxib)

Posted by DaveB on août 23, 2017

Sommer, Braun, Schröder, Kirschning, Synlett 2017 [10.1055/s-0036-1589097]

Late-Stage C–H Alkylation of Heterocycles and 1,4-Quinones via Oxidative Homolysis of 1,4-Dihydropyridines

Posted by DaveB on août 23, 2017

Gutiérrez-bonet, Remeur, Matsui, Molander, J. Am. Chem. Soc. 2017, 139(35), 12251-12258 [10.1021/jacs.7b05899]

Carboxylation of Aromatic and Aliphatic Bromides and Triflates with CO2 by Dual Visible Light – Nickel Catalysis

Posted by DaveB on août 21, 2017

Meng, Wang, König, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201706724]

Recent Advances in Asymmetric Hydrogenation of Tetrasubstituted Olefins

Posted by DaveB on août 21, 2017

Kraft, Ryan, Kargbo, J. Am. Chem. Soc. 2017, 139(34), 11630-11641 [10.1021/jacs.7b07188]

Causes and Significance of Increased Compound Potency in Cellular or Physiological Contexts

Posted by DaveB on août 19, 2017

Schwaid, Cornella-taracido, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00762]

Convergent Routes to Pyrroles Exploiting the Unusual Radical Chemistry of Xanthates – An Overview

Posted by DaveB on août 18, 2017

Quiclet-sire, Zard, Synlett 2017 [10.1055/s-0036-1590809]

Chemoselective Continuous Ru-Catalyzed Hydrogen-Transfer Oppenauer-Type Oxidation of Secondary Alcohols

Posted by DaveB on août 18, 2017

Labes, Battilocchio, Mateos, Cumming, De Frutos, Rincón, Binder, Ley, Org. Process Res. Dev. 2017, 21(9), 1419-1422 [10.1021/acs.oprd.7b00190]

Copper-Catalyzed Asymmetric 1,2-Addition of Grignard Reagents to 3-Acyl 2H-chromenes

Posted by DaveB on août 17, 2017

Calvo, Minnaard, Synlett 2017 [10.1055/s-0036-1588532]

Rh(III)-Catalyzed C–H Cyclization of Arylnitrones with Diazo Compounds: Access to 3-Carboxylate Substituted N -Hydroxyindoles

Posted by DaveB on août 17, 2017

Li, Li, Wu, Zhou, Liu, J. Org. Chem. 2017, 82(17), 8984-8994 [10.1021/acs.joc.7b01393]

Synthesis of Cyanamides from Cyanogen Bromide under Mild Conditions through N-Cyanation of Allylic Tertiary Amines

Posted by DaveB on août 17, 2017

Liang, Bao, Du, Zhang, Pang, Sun, Synlett 2017 [10.1055/s-0036-1588533]

Sequential Functionalizations of Carbohydrates Enabled by Boronic Esters as Switchable Protective/Activating Groups

Posted by DaveB on août 17, 2017

Mancini, Lee, Taylor, J. Org. Chem. 2017, 82(17), 8777-8791 [10.1021/acs.joc.7b01605]

Palladium-Catalyzed Arylation of Benzylic C–H Bonds of Azaarylmethanes with Aryl Sulfides

Posted by DaveB on août 17, 2017

Gao, Yamamoto, Nogi, Yorimitsu, Synlett 2017 [10.1055/s-0036-1589098]

C−H Bond Trifluoromethylation of Arenes Enabled by a Robust, High-Valent Nickel(IV) Complex

Posted by DaveB on août 16, 2017

D’accriscio, Borja, Saffon-merceron, Fustier-boutignon, Mézailles, Nebra, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201706237]

Continuous Flow Synthesis of Morpholines and Oxazepanes with Silicon Amine Protocol (SLAP) Reagents and Lewis Acid Facilitated Photoredox Catalysis

Posted by DaveB on août 16, 2017

Jackl, Legnani, Morandi, Bode, Org. Lett. 2017, 19(17), 4696-4699 [10.1021/acs.orglett.7b02395]

Selectivity Control in Ruthenium(II)-Catalyzed C–H/N–O Activation with Alkynyl Bromides

Posted by DaveB on août 15, 2017

Huang, Nakanowatari, Ackermann, Org. Lett. 2017, 19(17), 4620-4623 [10.1021/acs.orglett.7b02247]

Redox-Neutral Manganese(I)-Catalyzed C−H Activation: Traceless Directing Group Enabled Regioselective Annulation

Posted by DaveB on août 15, 2017

Lu, Greßies, Cembellín, Klauck, Daniliuc, Glorius, Angew. Chem. Int. Ed. 2017 [10.1002/anie.201707396]

A Chlorinating Reagent Yields Vinyl Chlorides with High Regioselectivity under Heterogeneous Gold Catalysis

Posted by DaveB on août 15, 2017

Liang, Ebule, Hammond, Xu, Org. Lett. 2017, 19(17), 4524-4527 [10.1021/acs.orglett.7b02101]

Direct Aldehyde C–H Arylation and Alkylation via the Combination of Nickel, Hydrogen Atom Transfer, and Photoredox Catalysis

Posted by DaveB on août 14, 2017

Zhang, Macmillan, J. Am. Chem. Soc. 2017, 139(33), 11353-11356 [10.1021/jacs.7b07078]

Sodium Diisopropylamide in Tetrahydrofuran: Selectivities, Rates, and Mechanisms of Alkene Isomerizations and Diene Metalations

Posted by DaveB on août 14, 2017

Algera, Ma, Collum, J. Am. Chem. Soc. 2017, 139(33), 11544-11549 [10.1021/jacs.7b05218]

The Current State of Peptide Drug Discovery: Back to the Future?

Posted by DaveB on août 11, 2017

Henninot, Collins, Nuss, J. Med. Chem. 2017 [10.1021/acs.jmedchem.7b00318]

Stoichiometric and Catalytic Aryl–Perfluoroalkyl Coupling at Tri-tert-butylphosphine Palladium(II) Complexes

Posted by DaveB on août 11, 2017

Ferguson, Bour, Canty, Kampf, Sanford, J. Am. Chem. Soc. 2017, 139(34), 11662-11665 [10.1021/jacs.7b05216]

Palladium-Catalyzed Negishi Coupling of α-CF3 Oxiranyl Zincate: Access to Chiral CF3 -Substituted Benzylic Tertiary Alcohols

Posted by DaveB on août 10, 2017

Zhang, Buchwald, J. Am. Chem. Soc. 2017, 139(33), 11590-11594 [10.1021/jacs.7b06630]

Copper-Mediated Synthesis of Monofluoro Aryl Acetates via Decarboxylative Cross-Coupling

Posted by DaveB on août 09, 2017

Fahandej-sadi, Lundgren, Synlett 2017 [10.1055/s-0036-1588516]

Chemical Synthesis of Oligosaccharides Related to the Cell Walls of Plants and Algae

Posted by DaveB on août 09, 2017

Kinnaert, Daugaard, Nami, Clausen, Chem. Rev. 2017, 117(17), 11337-11405 [10.1021/acs.chemrev.7b00162]

Rh/SPO-WudaPhos-Catalyzed Asymmetric Hydrogenation of α-Substituted Ethenylphosphonic Acids via Noncovalent Ion-Pair Interaction

Posted by DaveB on août 09, 2017

Yin, Chen, Li, Dong, Zhang, Org. Lett. 2017, 19(16), 4375-4378 [10.1021/acs.orglett.7b02098]

Transition-Metal-Free Decarboxylative Iodination: New Routes for Decarboxylative Oxidative Cross-Couplings

Posted by DaveB on août 08, 2017

Perry, Quibell, Panigrahi, Larrosa, J. Am. Chem. Soc. 2017, 139(33), 11527-11536 [10.1021/jacs.7b05155]

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